Ochem Spring PHYS 10164
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This 0 page Class Notes was uploaded by Veronica Morgan on Wednesday February 3, 2016. The Class Notes belongs to PHYS 10164 at Texas Christian University taught by Dr. Dobrovolny in Spring 2016. Since its upload, it has received 25 views. For similar materials see General Physics II in Physics 2 at Texas Christian University.
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Date Created: 02/03/16
CHEMISTRY 30143 Laboratory Report Form Name Veronica Morgan Date February 8 2016 Unknown Code Number A33 Identity of Unknown 355trimethyl1hexanol Physical State liquid 1 Physical Constants a Observed b Lit Value BP range 183C 186C 2 Solubility Tests soube insoube Water 5 NaOH 5 NaHCO 5HCI Conc H 2 Ether 3 SO 4 Not used Not used Solubility Classi cation N 3 Classi cation and Subclassi cation Tests Name of Test Speci c Observations lnferences Cerium Ammonium Nitrate Development of red complex Performed in the last hour of lab so a change from red to cooress was not witnessed test for acohos Chromic Anhydride Oxidation Jones Development of a bluegreen color in 3 Test seconds test for a primary or secondary acoho odoform Test No development of a yellow precipitate test for secondary methyl carbino Lucas Test Unknown was not soluble in the reagent therefore more than 6 carbons in the structure 4 Compound Name Compound Name Boiling Point Reason for Ruling Out 1octanol 23dichloro1propanol Ruled out because has less than 6 carbons in structure 355trimethyllhexanol 2ethyl1hexanol 12propanediol Ruled out because has less than 6 carbons in structure cyclohexylmethanol 22methoxyethoxyethanol Ruled out because has less than 6 carbons in structure tetrahydrofurfuryl alcohol Ruled out because has less than 6 carbons in structure 2octanol Ruled out because iodoform test was negative for secondary methyl carbonyl 5 Re ned List Compound Name Boiling Point Name of Derivatives and MP 1octanol 355trimethyllhexanol 2ethyl1hexanol cyclohexylmethanol 6 Preparation of Derivative Name of Derivative Observed MP Range Literature MP and Reference 35dinitrobenzoate 6061 62 7 Conclusion
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