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Fund of Organic Chemistry I

by: Dominic Kling

Fund of Organic Chemistry I CHEM 3331

Marketplace > University of Houston > Chemistry > CHEM 3331 > Fund of Organic Chemistry I
Dominic Kling
GPA 3.71

Thomas Albright

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Thomas Albright
Class Notes
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This 7 page Class Notes was uploaded by Dominic Kling on Saturday September 19, 2015. The Class Notes belongs to CHEM 3331 at University of Houston taught by Thomas Albright in Fall. Since its upload, it has received 17 views. For similar materials see /class/208156/chem-3331-university-of-houston in Chemistry at University of Houston.


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Date Created: 09/19/15
Identification of Organic Compounds A Chromatography separation of a mixture 1 preparative high performance liquid Chromatography HPLCa 10 min 2 analytical gas chromatography GC B Mass spectroscopy MS gives molecular weight osometimes combined with G0 GCMS Chapter 12 Negatively Low moxecular weugm mns are asnecma on much and Mn the wall The Incoming electron and he exacted mm 0 j o Wclnnexane 34 Dmynrm a a 4 a cm may min4 mm m 4 M e 2e M gt chuaym A they will give different fragmentation patterns A hlgnrenergy The residual M H t leclron ad 2 2 cal cation quotWe will not worry about this Chapter 12 3 5 o Rme ive abundance 40 50 60 7o 50 90 100 110 120 He a ve abundance 1139 60 3970 ll 90 With sophisticated MS equipment exact masses can be determined ie 100 110 120 CeHm C5HEO 6 16 s X 12000 72000 5 20 5 X 12000 snnoo 12 H12gtlt 1005 096 B 1H 96 1 50 molCGH13 Chapter 1 2 With exact masses we can determine the molecular formula CVHWOXN ClZ where x y etc are whole numbers It is also useful to determine the degree of unsaturation degree of unsaturation Z number of double bonds number of rings Z O CnH2n2 alkane 1 CnH2n alkene or cycloalkane 2 CnH2n2 alkyne or diene or bicycloalkane Z 1220 2 H where C of carbons H of hydrogens count 0 atoms as zero count N atoms as one half of a carbon atom for halogens count as H Chapter 12 C Infrared Spectroscopy IR tells about the functional groups in a molecule lt gt 300 300430 3071 10 10 5 J Energy ow Frequencyv HZ 1 14 Stretching vibrations 101 1 1o16 0 10 2 10W quot 05 7 Rys ultraviolet v rays I x t 10 10 1o 4 Microwaves a o vgyes g I I Bending vibrations 539 14 10 1o 2 1 Wavelength cm C symmetri inplane bend scissor asymmetric invplane bend rock Solvent cell D et ecto r ou rc e of radiiatfon So lvem plus sample cell


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