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Organic Chemistry II lab manual

by: Kathleen Quijada

Organic Chemistry II lab manual CHM 2211L

Marketplace > Florida International University > Chemistry > CHM 2211L > Organic Chemistry II lab manual
Kathleen Quijada
GPA 3.46
Organic Chemistry II Lab manual

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Hello! This is my whole lab manual for organic chemistry! The professor is Dr. Becker, but the lab was with TA Nan Fang. Enjoy!
Organic Chemistry II Lab manual
FIU organic chemistry II Lab manual
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This 84 page Reader was uploaded by Kathleen Quijada on Saturday January 31, 2015. The Reader belongs to CHM 2211L at Florida International University taught by Becker in Fall2014. Since its upload, it has received 42 views. For similar materials see Organic Chemistry II Lab manual in Chemistry at Florida International University.


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Date Created: 01/31/15
l KCL H tlfJ f lPentherlD Date UNKNOWN Preliminary Identification 20 points You have been given an unknown compound In the first part of this lab you will examine the phyeical properties solubility and elemental analysis of the unknown Fill out the information below as best as possible A successful determination of the functional group in your unknown compound is dependent upon the following examinations You will be graded on how accurate and diligent you perform At the final step you must predict two potential functional groups that your compound might contain AND explain your reason for choosing that functional group DO NOT SEPARATEJ39I EAR THE PAGES OF UNKNOlW EXAMINATION I 1 Unknown number l V 1 Physical properties 5 points S A Solid or liquid r v Color Ignition test Flammability 7 quot Manner of melting 7 Odor of gases ll 2 535quot Beilstein test testing for halogens e39quot Melting paint 7 u a 739 Boiling point 2 Solub fnr 5 points H20 5 or 10 HGI Suit or 10 Nad H 39l 5 oriot u NaHG g N v Reactivity 1with H2504 231 Unknawn I 232 Preliminanf Iden ti m un Elemental Analysis SodiUm Fusion 5 points Nitragen Chlorine AL Tiff e 1 L 39 n 1 l a V 7 F f t a 2 x quot 1 39 a f l 4 39 k 1 a i J 1 Liarquot 39 Ij 1 E I rquot 39 fair 37quot rquot r j T 4 41 f L 1 Jr a n 4 w w l a 3955 L J lm Zi h wLQ U M K N o w M Dam Ht Final Examination 20 points In the second part of the unknown lab you will rst isolate which functional group oi the two you predicted is present You quotwill then prepare derivatives of your unknown in an attempt to identify the actual unkuo m i Compound Fill out the information below as best as possible You will be graded on how accurate your answers are for your unknowns At the i ial step you must identify your un lmorm compound DO NOT SEPARATEJTEAR PAGES OF THE UNKNOWN EXAMINATION u 139 Narrowing your functional group 5 points Give the details as to what tests you did to narrow your iuuetiooal group including Unknown number quot7 whether it s 1 2quot or 3 as ior aminesialoohols S U S welt17 i1 Ci 9 unitiiquot 1S 5 fquot C writ ii Ci lu l i or 2 Derivative 1 5 points Reagent used a Names of predicted derivative compound5 and their melting pointis no 39 rumK i iji if l at i lt1 C39 ir39u r Piersxii h J I Cri o uo 2 a is i o i i m ora go Experimentalr lting point quot l L 233 Unknown 1 39 234 Final Emmina en 3i Derivative 2 5 points Reagent used Predicted derivative compound 7 Predicted derivative compound meitmg point 7 i Experimentai melting point Name your quot knpwn Compound 5 Bernref H Wm v f U jHXL Dl L M ElliP NUMBER E quotHIquot EN WSUBJECT 7 r A TE i E if Xfigwltw Cw U f39lgd a 2611 Of M Z7 12 Mg I I v quotZED H LUIGKERJDESK MD I H N mlawmon 00ijan 35qu quot Z mm i 8T quotViir 4 Emma 54 1226 cm 80 fw f MHZ A913 lq bw U M 613 1 56 39 014 quot4i 5 sp r in M 1 w I Ur p lt3 6 rm if I me aims r6 39 PU f ih u aw i V EH T Q SW haw meuN HM 1110 9p L quotFEWE tame M Qx39plmimwmi In bbi am 5 r quot 39 I 1 a y r13 1 f p Q 161 i ewxjg m P O 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predict two potential functional groups that your compound might contain AND explain YOULIL reason ior Choosing that functional group DO NOT SEPARATEITEAR 39l HE PAGES 01F UNKNOWN EXAMINATION ii 1 PhySiCai properties 5 points I i A Solid or liquid 7 39 Ulv cam l l lt1 W mono ignition teat J V Flammability 6 b lr 39 m Manner of melting Uquot CM J Odor of gases 7 I a Beilsteintest testing for halogens WGLUCi l39mfjam Melting point I V Boiling point C 2 Solubility 5 points Unknown number H H2O I 59in or Hm I 5 or 19 MaoH I 5 HalliICE inmth 3 Bl 1m M l Sol ulDUL Reactivity with H2304 235 Unknown 2 Preliminary Identi catinn F 3 Eiementai Analysis Sodium Fusion 5 points I Nitrogen BhloriV Bromine i quot yfr ffi 39 I I rquotva 7 7 x L 4 Predictions of ctionai group presenf and reasoning why 5 points 11 I W kME iquot CA 90931 big p39rtditdi r1 bQCCLUS H 2 Semi in M So HI H H 3 wow I r v QtSSlBKsz gt W9 236 2 w ame KEXHWKW U N M 0 W N 39 pantherlo Daie J z i Final Examination 20 points in the second part of the unknown lab you will first isolate which functional group of the two you predicted is present You will then prepare 2 derivatives oi your unknown in an attempt to identity the actual unknown compound Fill out the iniorrnation beiow as best as possible You will be graded on how accurate your answers are for your unknown At the nal step you must identify your unknown compound 0 NOT SEPARATEXTEAR THE PAGES OF UNKNOWN EXAMINATION Unknown number i 1 Narrowing your functional group 5 points Give the details as to what tests you did to narrow your functional group including whether it s 1 2 or 3 as for aminesalcohoisyl an tamuse 3 at p itsgt5er PmeiLc oi i because a was Samoa 391 n H a so fia A ti e m s 446 gee Luigi gig gisee atomkeg iiquot gi C ca result I great i it was ta Gimme i i 2 Derivative 1 5 points Reagent used 5554 29M 5 U i g 1 Lin Kort 4 D 39 Predicted derivative compound 9 m G Predicted derivative compound meiting point i i 17L l I Experimental 7 Boil 39 int no to o mi aC 237 Unknawn 2 Final Examimtian 3 Analysis of TH NMH match the peaks with your functional group 5 points On the attached 1HISJ IVIIR spectrum draw the Structure of your compound and assign the peaks to the appropriate pmtons 4 Name your unknown compnund 539 points i quot a h 39r f 39 39 u Pa Jar P x z I I r I K W quot 39 xquot t I x i I a la MJ H I g I 391 39 39 39 z r 238 KanHth em Oui39j a dg quot 3ff 7q HM UNKNOWN 18 CHDCHE 200 150 gt 1759 120 V r mo 7 BO 7 BU 4D 7 20 r D MM 4 39 19E i f 1iquot I V V 7 7 2 w r Yawn u aquot 39I r m a I i h 1 9 v Ice Quit 2 a 7 0L i e 0 f amqw if I 39 x 20 9K CrayL t E SBLE A an N694 Qu Zi FQ CmuaAq 7 e ngg7 L1 u i 5 LN r L4 502 W J 39 5 Wwairmbm ea UVWWM 1wij E E quot Riot pure e Qg rh I 39 f amp 39 x a39 Rmd mampMMV e 7 rr 6 ea 1 I I Z 7 J r 39 39 In 7 m m Hm 739 Ea Ii1quot p 7 fig Ex Eli a j fa 39l n Age H f quot V W 7quot LI 5 h 139 47 7 m a m f f e E M 39 7 a m d C 1 by m 7 if r g I UL Lu m s Ara 3 Wait UH 102369 quotm k J U 39 v If 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