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Suppose you have just synthesized heptanoic acid from heptan-1-ol. The product is

Chapter 20, Problem PROBLEM 20-4

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QUESTION:

Suppose you have just synthesized heptanoic acid from heptan-1-ol. The product is contaminated by sodium dichromate, sulfuric acid, heptan-1-ol, and possibly heptanal. Explain how you would use acid–base extractions to purify the heptanoic acid. Use a chart, like that in Figure 20-3, to show where the impurities are at each stage.

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QUESTION:

Suppose you have just synthesized heptanoic acid from heptan-1-ol. The product is contaminated by sodium dichromate, sulfuric acid, heptan-1-ol, and possibly heptanal. Explain how you would use acid–base extractions to purify the heptanoic acid. Use a chart, like that in Figure 20-3, to show where the impurities are at each stage.

ANSWER:

Step 1 of 2

From the given data,

Sodium dichromate, sulfuric acid, 1-heptanol and heptanal are impurities. The mixture is shaked with ether/water.

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