An article in the Materials Research Bulletin [1991, Vol.

Chapter 13, Problem 12E

(choose chapter or problem)

An article in the Materials Research Bulletin [1991, Vol. 26(11)] investigated four different methods of preparing the superconducting compound \(\mathrm{PbMo}_{6} \mathrm{~S}_{8}\). The authors contend that the presence of oxygen during the preparation process affects the material’s superconducting transition temperature \(T_{\mathrm{c}}\). Preparation methods 1 and 2 use techniques that are designed to eliminate the presence of oxygen, and methods 3 and 4 allow oxygen to be present. Five observations on \(T_{\mathrm{c}}\) (in \({ }^{\circ} \mathrm{K}\)) were made for each method, and the results are as follows:

(a) Is there evidence to support the claim that the presence of oxygen during preparation affects the mean transition temperature? Use \(\alpha=0.05\)

(b) What is the \(P \text {-value }\)  for the \(F \text {-test }\) in part (a)?

(c) Analyze the residuals from this experiment.

(d) Find a \(95 \%\) confidence interval on mean \(T_{\mathrm{c}}\) when method 1 is used to prepare the material.

Equation Transcription:

       

   

     

       

Text Transcription:

PbMo6S8      

Tc  

Tc    

°^K  

\alpha =0.05

P-value

F-test

95%

Tc      

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